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leap HPLC sample vials lab efficiency

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Analytical HPLC System: Preparative HPLC System: High-Throughput HPLC System: Preparative HPLC System: Flow Rate: up to 5 mL/min with , ; 0.2 to 10 mL/min with , , : 0.05 to 5 mL/min with ; 0.2 to 10 mL/min with , , : 4-50 mL/min: up to 5 mL/min: 1-200 mL/min: Max. Pressure: up to 800 bar

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Reactions were carried out in autosampler vials with incubation in a thermostatted CE autosampler tray. MECC was performed using borax buffer (17.5 mM, pH 9.3) modified with sodium dodecyl sulfate (70 mM). Repetitive injections were made from the sample vial throughout the course of the reactions at a frequency of up to 10 h-1.

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Deterioration is more evident in higher efficiency columns. For example, a 3 micron packing retained by 0.5 micron frits is more susceptible to plugging than a 5 or 10 micron packing retained by 2 micron or larger frits. Proper column protection and sample preparation are essential to getting the most from each column.

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