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Place 3 mL of each of the 3 standards into 3 analysis vials and cap the vial with a rubber septum. Place the standards vials in a water bath held at 50 °C for 20 minutes. Take 250 mL of the headspace above the liquid by inserting the needle into the cap (whilst still in the bath) and manually inject into the GC. Obtain a chromatogram.
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